Instrumentation and Equipment

Spectroscopy

NMR

Agilent V500 WB

500 MHz solid-state MAS-NMR with 1,6-, 3,2- und 6 mm as well as continuous flow probes and VT-unit

FT-IR

Jasco FT/IR 4100

Infrared spectrometer with (diamond-)ATR and ht/hp- and lt-DRIFT accessory

UV-Vis

Jasco V-650

Dual beem UV-Vis-spectrometer variable temperature, stirred sample holder and DRUV-option

Adsorption

N2-physisorption

Micromeritics ASAP 2010

volumetric measurement of sorption isotherms at 77 K up to 1 atm. Determination of BET-areas and pore volumes.

Gassorption

Micromeritics ASAP 2010C

volumetric measurement of sorption isotherms of gaseous alkanes / alkenes at 0 – 40 °C up to 1 atm.

Magnetic suspension balance

Rubotherm IsoSORP

gravimetric measurement of sorption isotherms from 77 to 325 K up to 150 bar.

Dynamic vapor sorption

Surface Measurement Systhems DVS-ET

dynamic gravimetric measurement of (water) vapor sorption isotherms

PSA

L&C PSA-300LC

two column pressure swing adsorption apparatus

X-ray Diffraction

Powder XRD

PANalytical Emryrean

Powder diffractometer with PIXcel3D 1×1 Detector und Reaction-/low temperature- and controlled humidity chambers.

Thermal Analysis

STA

Netzsch STA 449 F3 Jupiter

Simultaneous thermogravimetric and calorimetric analysis under regulated steam atmosphere.

Gaschromatography

GC

Bruker 450/460 GC

Gaschromatographs for online / offline analyses with liquid / gas Injectors and FID / TCD

GC/MS

Bruker Scion GC/MS

Gaschromatograph with mass spectrometer