Instrumentation and Equipment

Spectroscopy

NMR
Agilent V500 WB
500 MHz solid-state MAS-NMR with 1,6-, 3,2- und 6 mm as well as continuous flow probes and VT-unit
FT-IR
Jasco FT/IR 4100
Infrared spectrometer with (diamond-)ATR and ht/hp- and lt-DRIFT accessory
UV-Vis
Jasco V-650
Dual beem UV-Vis-spectrometer variable temperature, stirred sample holder and DRUV-option

Adsorption

N2-physisorption
Micromeritics ASAP 2010
volumetric measurement of sorption isotherms at 77 K up to 1 atm. Determination of BET-areas and pore volumes.
Gassorption
Micromeritics ASAP 2010C
volumetric measurement of sorption isotherms of gaseous alkanes / alkenes at 0 – 40 °C up to 1 atm.
Magnetic suspension balance
Rubotherm IsoSORP
gravimetric measurement of sorption isotherms from 77 to 325 K up to 150 bar.
Dynamic vapor sorption
Surface Measurement Systhems DVS-ET
dynamic gravimetric measurement of (water) vapor sorption isotherms
PSA
L&C PSA-300LC
two column pressure swing adsorption apparatus

X-ray Diffraction

Powder XRD
PANalytical Emryrean

Powder diffractometer with PIXcel3D 1×1 Detector und Reaction-/low temperature- and controlled humidity chambers.

Thermal Analysis

STA
Netzsch STA 449 F3 Jupiter

Simultaneous thermogravimetric and calorimetric analysis under regulated steam atmosphere.

Gaschromatography

GC
Bruker 450/460 GC

Gaschromatographs for online / offline analyses with liquid / gas Injectors and FID / TCD

GC/MS
Bruker Scion GC/MS

Gaschromatograph with mass spectrometer